Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cumen hydroperoxide | HCID 53627471 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Phenol Acetone | HCID 54464289 | — |
Reaction Steps
To a 250-ml round bottom flask fitted with a condenser, heater, stirrer and feed control, is charged a mixture of 60.0 g of acetone and 0.1 g of Engelhard Clay-24. The mixture is heated to reflux (57° C.) with stirring, and 40.0 g of "80%" cumene hydroperoxide solution added dropwise such that the pot temperature does not exceed 66° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04898987 |
|---|
| Source dataset | uspto-grants-1990_02 |
|---|
| ORD ID | ord-a5d0b21d11564afebfe6a91fc462c4fe |
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| Source note | uspto-grants-1990_02 |
|---|
