HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14261123, compound → HCID 14261125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14261123 | HCID 14261123 | — |
| Solvent | Butylamine | HCID 8007 | — |
| Product | HCID 14261125 | HCID 14261125 | — |
Reaction Steps
24.9 g (0.09 mol) of 5(S)-azido-6-cyclohexyl-2(S)-isopropyl-4(S)-hexanolide in 250 ml of n-butylamine are boiled under reflux for 10 hours. After evaporating off the solvent, the residue is recrystallised from hexane: m.p. 100°-100.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04898977 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-d9d754a9d42944e49e9433e3eabfade8 |
| Source note | uspto-grants-1990_02 |