HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl isocyanate → HCID 14627711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl isocyanate | HCID 61277 | — |
| Reactant | (+)-7,8-dihydro-6,6-dimethyl-7-hydroxy-8-amino-6H-pyrano[2,3-f]benz-2,1,3-oxadiazole | HCID 11107308 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14627711 | HCID 14627711 | 44% |
Reaction Steps
To a mixture of 200 mg (0.850 m mol) of 7,8-dihydro-6,6-dimethyl-7-hydroxy-8-amino-6H-pyrano [2,3-f] benzo-2,1,3-oxadiazole and 20 ml of dichloromethane were added 92 μl (0.935 m mol) of isopropyl isocyanate with stirring at the room temperature, followed by stirring for 6 hours. The precipitated crystals were filtered off to obtain 120 mg (yield: 44%) of the intended compounds as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04900752 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-58755cedc6594ae7a51da9275e987bb6 |
| Source note | uspto-grants-1990_02 |