m-Chloroperbenzoic acid → HCID 15059459, compound

Participants

Reaction Steps

The product of step (a) above (750 mg) in ethyl acetate (7 ml) was cooled to -10° and treated with a solution of m-Chloroperbenzoic acid (660 mg) in ethyl acetate (4 ml). After 1 hour the solution was washed with sodium bicarbonate solution, sodium bisulphate solution and brine then dried and evaporated. The residue was flash chromatographed (ethyl acetate) to produce the subtitle compound as a clear oil MS (FAB) M+1 at 248 bp 232.

Provenance & Evidence