Ethyl Acetate → HCID 178493115, compound

Participants

Reaction Steps

The product of step (c) above (103 mg) was dissolved in ethyl acetate (7.5 ml) and stirred at -10° . A solution of m-chloroperbenoic acid (58 mg of 85%) in ethyl acetate (0.5 ml) was added and the mixture stirred for 50 minutes. The solution was washed with sodium bicarbonate solution, sodium bisulphite solution, water and brine then dried and evaporated. After trituration with ether the solid was dried to afford the title compound. MS (FAB) M+1 at 380.

Provenance & Evidence