HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 19866663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 19866712 | HCID 19866712 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 19866663 | HCID 19866663 | — |
Reaction Steps
The product of step (c) above was dissolved in ethyl acetate (100 ml) and cooled to -10°. m-Chloroperbenzoic acid (2.98 g) was added and after 1.5 hour the mixture was worked-up then chromatographed (ethyl acetate) to give the sub-title compound as a solid, mp 103°-105°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04900751 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-7a3e757582a046f29bbc066809eabf2a |
| Source note | uspto-grants-1990_02 |