Hydrochloric Acid → HCID 14989649, compound

HRID 1199674Notes

Reaction equation

HRID 1199674 reaction equation
[C:1]1([S:7]([NH:10][C:11]2[CH:12]=[CH:13][C:14]([CH2:17][CH2:18][CH2:19][C:20]([O:22]C)=[O:21])=[N:15][CH:16]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Na+].Cl>C(O)C>[C:1]1([S:7]([NH:10][C:11]2[CH:12]=[CH:13][C:14]([CH2:17][CH2:18][CH2:19][C:20]([OH:22])=[O:21])=[N:15][CH:16]=2)(=[O:9])=[O:8])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 14989648HCID 14989648, compound

Product 1

HCID 14989649HCID 14989649, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of methyl 4-(5-benzenesulphonamidopyrid-2-yl)-butanoate (1.3 g, 4.2 mmole) in ethanol (25 ml) and 10% w/v sodium hydroxide solution (10 ml) was stirred for 1 hour. The solution was treated with hydrochloric acid and the precipitate was collected by filtration.

Workup

  1. filtrationthe precipitate was collected by filtration

Sources & evidence

ORD record
ord-5bd7e1d8ad834ae4998daa3ea0ee487e
Source dataset
uspto-grants-1990_02
Patent number
US04902698

Reaction notes

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