Ethanol → HCID 19865487, compound

Participants

Reaction Steps

A solution of 3-benzenesulphonamido-2-(3-cyanopropyl)pyridine (5.22 g) in ethanol (100 ml) and 15% w/v sodium hydroxide solution (50 ml) was refluxed for 6 hours. The pH of the solution was adjusted to pH=4 when a white solid precipitated from the solution. The solid was collected by filtration and recrystallised from ethanol to give the title compound (3.34 g) as white needles. m.p. 156°-157° C.

Provenance & Evidence