Hydrochloric Acid → HCID 14989663, compound

Participants

Reaction Steps

A solution of methyl 4-[5-(phenylsulphamoyl)pyrid-2-yl]butanoate (0.7 g), 10% w/v sodium hydroxide solution (5 ml) in ethanol (10 ml) was stirred for 1 hour. The solution was acidified with dilute hydrochloric acid (pH=3) and cooled. The precipitate was collected and recrystallised from ethanol to give the title compound as prisms (0.56 g). m.p. 158°-159° C.

Provenance & Evidence