HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 7986269, compound → 2-[2-(3-Hydroxyphenyl)ethyl]benzothiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 7986269 | HCID 7986269 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-[2-(3-Hydroxyphenyl)ethyl]benzothiazole | HCID 14051161 | 92% |
Reaction Steps
A mixture of 6.0 g of 2-(trans-3-hydroxystyryl) benzothiazole and 0.5 g of 5% palladium-carbon in 80 ml of ethanol was stirred under hydrogen gas stream under normal pressure at 50° to 60° C. for 3 hours. After completion of the reaction, the catalyst was filtered off and the filtrate was evaporated under reduced pressure to obtain 5.5 g (yield 92%) of the title compound as pale gray crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04902700 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-5681bb550444475ca7f3f7878af95cdd |
| Source note | uspto-grants-1990_02 |