HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54070531, compound → HCID 14051166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54070531 | HCID 54070531 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14051166 | HCID 14051166 | 90% |
Reaction Steps
An amount of 1.0 g of 2-(3-aminostyryl)-4-ethyl-5-methylthiazole and 200 mg of 5% palladium-carbon were added to 20 ml of ethanol and catalytic reduction was carried out in a hydrogen gas atmosphere at room temperature and normal pressure for 12 hours. After the reaction mixture was filtered, the solvent was evaporated under reduced pressure to give 0.90 g (yield 90%) of the title compound as pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04902700 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-ef96e926a1984d2298f1cdc66a0f23a8 |
| Source note | uspto-grants-1990_02 |