Methanol → HCID 86743765, compound

Participants

Reaction Steps

Into a solvent mixture of 6 ml of methanol and 1 ml of water were added 96 mg of N-methyl-D-glucamine and 200 mg of 2-[trans-3-(cis-2-carboxycyclohexanoyl)aminostyryl]benzothiazole and the mixture was stirred at room temperature for 30 minutes. After evaporation of the solvent under reduced pressure, the crude crystals formed were recrystallized from ethanol-ethyl ether to obtain 215 mg (yield 73%) of the title compound.

Provenance & Evidence