HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-dihydro-7-nitro-5-(o-chlorophenyl)-2H-1,4-benzodiazepine-2-thione → HCID 19865838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-dihydro-7-nitro-5-(o-chlorophenyl)-2H-1,4-benzodiazepine-2-thione | HCID 12371433 | — |
| Reactant | 2-Ethoxyacetohydrazide | HCID 14750209 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 19865838 | HCID 19865838 | — |
Reaction Steps
In the manner given in Example 1, a solution of 1,3-dihydro-7-nitro-5-(o-chlorophenyl)-2H-1,4-benzodiazepine-2-thione in n-butyl alcohol was heated to reflux with ethoxyacetic acid hydrazide to give 8-nitro-1-(ethoxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04902794 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-8351b0e761ca48699101f0dfdd70709b |
| Source note | uspto-grants-1990_02 |