HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 16641271, compound → HCID 19865766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 16641271 | HCID 16641271 | — |
| Reactant | HCID 19865778 | HCID 19865778 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 19865766 | HCID 19865766 | — |
Reaction Steps
In the manner given in Example 1, a solution of 1,3-dihydro-6-ethylsulfinyl-5-[p-(trifluoromethyl)phenyl]-2H-1,4-benzodiazepine-2-thione in n-butyl alcohol was heated to reflux with isopropoxyacetic acid hydrazide to give 7-ethylsulfinyl-1-(isopropoxymethyl)-6-[p-(trifluoromethyl)phenyl]-4H-s-triazolo[4,3-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04902794 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-e44cff40b7da4891b905400999a69594 |
| Source note | uspto-grants-1990_02 |