Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1199787Generated: October 31, 2026

2-Hydroxyacetohydrazide → HCID 86743766, compound

https://huagongshe.com/reaction/1199787

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-HydroxyacetohydrazideHCID 350536—
ReactantHCID 19865780HCID 19865780—
Solvent1-ButanolHCID 263—
ProductHCID 86743766HCID 86743766—

Reaction Steps

In the manner given in Example 11, a solution of 1,3-dihydro-8-(ethylsulfinyl)-6-(diethylamino)-5-(m-formamidophenyl)-2H-1,4-benzodiazepine-2-thione and hydroxyacetic acid hydrazide in n-butylalcohol was refluxed to give 9-(ethylsulfinyl)-7-(diethylamino)-1-hydroxymethyl)-6-(m-formamidophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04902794
Source datasetuspto-grants-1990_02
ORD IDord-aecc73d870de44a598ce08bc7f555a8a
Source noteuspto-grants-1990_02