HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 54472884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Styrene Oxide | HCID 7276 | — |
| Reactant | Methyl thiophene-3-ethylamine | HCID 19826895 | — |
| Product | HCID 54472884 | HCID 54472884 | — |
Reaction Steps
A solution of methyl thiophene-3-ethylamine (3.3 g) and styrene oxide (1.8 ml) in acetonitrile (17 ml) was heated under reflux for 24 hours. The mixture was evaporated and the residual oil chromatographed on silica eluting with 2% methanol in dichloromethane to give the title product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904653 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-5ccaff33a4604bc38b0a82ad5ff03cd9 |
| Source note | uspto-grants-1990_02 |