HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19864517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19864536 | HCID 19864536 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 19864517 | HCID 19864517 | 85.6% |
Reaction Steps
N-Acetyl-4-(2-methylimidazo[4,5-c]pyrid-1-yl)butylamine (1 g) was dissolved in 2M hydrochloric acid (100 ml) and heated at reflux for 8 hours. The solution was basified to pH8 with 2M sodium hydroxide solution and then extracted with methylene chloride using a continuous extractor. The organic extract was evaporated under vacuum to give the title product, (0.71 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904671 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-c3fdb42302eb4449aa08e36582e76702 |
| Source note | uspto-grants-1990_02 |