HRID1200197

反应详情

EQUATION

反应方程式

HRID 1200197 反应方程式

PROCEDURE

实验过程

A 50:50 weight ratio copolymer of alpha-methylstyrene and styrene is made by means of continuous anionic polymerization so as to have a 195,000 Mw and a Mw /Mn of 2.2. 2884.1 grams of the anionically polymerized copolymer are dried mixed with 941.1 grams of the grafted rubber/ungrafted rubber mixture from Example 2. The mixture is fed to a Baker Perkins MP mixer compounding line. The compounding section is operated at 400 rpm and the extruder is run at 110 rpm. The melt temperatures are 203°, 207°, 203° and 211° C. in zone 1, zone 2, the extruder and the die, respectively. The compounding line is fed at a rate of about 20 pounds per hour of polymer-rubber blend.

WORKUP

后处理

  1. custom2884.1 grams of the anionically polymerized copolymer are dried
  2. additionmixed with 941.1 grams of the grafted rubber/ungrafted rubber mixture from Example 2
  3. customare 203°, 207°, 203° and 211° C. in zone 1, zone 2