HuagongsheHuagongshe Chemistry Print Report · For research reference only
Alpha-Methylstyrene → Benzene, ethenyl-, polymer with (1-methylethenyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Alpha-Methylstyrene | HCID 7407 | — |
| Reactant | Styrene | HCID 7501 | — |
| Product | Benzene, ethenyl-, polymer with (1-methylethenyl)benzene | HCID 165735 | — |
Reaction Steps
A 50:50 weight ratio copolymer of alpha-methylstyrene and styrene is made by means of continuous anionic polymerization so as to have a 195,000 Mw and a Mw /Mn of 2.2. 2884.1 grams of the anionically polymerized copolymer are dried mixed with 941.1 grams of the grafted rubber/ungrafted rubber mixture from Example 2. The mixture is fed to a Baker Perkins MP mixer compounding line. The compounding section is operated at 400 rpm and the extruder is run at 110 rpm. The melt temperatures are 203°, 207°, 203° and 211° C. in zone 1, zone 2, the extruder and the die, respectively. The compounding line is fed at a rate of about 20 pounds per hour of polymer-rubber blend.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904730 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-56cbeb86ab3b42d390b1edb433e7fda8 |
| Source note | uspto-grants-1990_02 |