Phenol → HCID 19865004, compound

HRID 1200278Notes

Reaction equation

HRID 1200278 reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:8][C:9](=[CH2:17])[CH2:10][CH2:11][CH2:12][C:13]([O:15][CH3:16])=[O:14]>>[OH:7][C:1]1[CH:6]=[CH:5][C:4]([C:9]([CH3:17])([CH3:8])[CH2:10][CH2:11][CH2:12][C:13]([O:15][CH3:16])=[O:14])=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 996PhenolHCID 642298methyl 5-methylhex-5-enoate

Product 1

HCID 19865004HCID 19865004, compound

Procedure

94 Parts of phenol, 14.2 parts of methyl 5-methyl-hex-5-enoate, and 5.0 parts of Fulmont 237® were stirred at 110° C. for 20 hours. The partly cooled reaction mixture was then filtered free of catalyst and distilled. After recovering 82 parts of phenol there was obtained methyl 5-(4-hydroxyphenyl)-5-methyl-hexanoate b0.85 167°-72° C. with the following percentage composition by weight.

Workup

  1. customThe partly cooled reaction mixture
  2. filtrationwas then filtered free of catalyst
  3. distillationdistilled
  4. customAfter recovering 82 parts of phenol

Sources & evidence

ORD record
ord-6fb878ba45524af38c84d7aaea0facdb
Source dataset
uspto-grants-1990_02
Patent number
US04904815

Reaction notes

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