HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 19865004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | methyl 5-methylhex-5-enoate | HCID 642298 | — |
| Product | HCID 19865004 | HCID 19865004 | — |
Reaction Steps
94 Parts of phenol, 14.2 parts of methyl 5-methyl-hex-5-enoate, and 5.0 parts of Fulmont 237® were stirred at 110° C. for 20 hours. The partly cooled reaction mixture was then filtered free of catalyst and distilled. After recovering 82 parts of phenol there was obtained methyl 5-(4-hydroxyphenyl)-5-methyl-hexanoate b0.85 167°-72° C. with the following percentage composition by weight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904815 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-6fb878ba45524af38c84d7aaea0facdb |
| Source note | uspto-grants-1990_02 |