HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perchloric Acid → HCID 19864935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perchloric Acid | HCID 24247 | — |
| Reactant | 2-Octene, 8-butoxy-2,6-dimethyl- | HCID 116735 | — |
| Reactant | HCID 19865004 | HCID 19865004 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19864935 | HCID 19864935 | — |
Reaction Steps
10.3 Parts of 4-(5-methoxycarbonyl-2-methyl-pent-2-yl)-phenol, 4.2 parts of citronellyl n-butyl ether, and 0.5 parts of 70% perchloric acid in 25 parts of methylene chloride were stored at room temperature for 4 days. The work-up followed Example 61 and gave on distillation 2-(8-n-butyloxy-2,6-dimethyl-oct-2-yl)-4-(5-methoxycarbonyl-2-methyl-pent-2-yl)-phenol with b0.8, 228°-36° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904815 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-664e152e28794d879218371f1174bf46 |
| Source note | uspto-grants-1990_02 |