HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perchloric Acid → HCID 19865037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perchloric Acid | HCID 24247 | — |
| Reactant | Phenol, p-decyl- | HCID 572479 | — |
| Reactant | methyl 5-methylhex-5-enoate | HCID 642298 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19865037 | HCID 19865037 | — |
Reaction Steps
2.3 Parts of 4-n-decylphenol, 1.4 parts of methyl 5-methyl-hex-5-enoate, 0.25 of 70% perchloric acid, and 10 parts of methylene chloride were stored for 12 days at room temperature. The work up followed Example 61 and gave on distillation, methyl 5-(5-n-decyl-2-hydroxyphenyl)-5-methyl-hexanoate, b0.8, 160°-7° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904815 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-2cff0c88e9064de3986b1b02394e1129 |
| Source note | uspto-grants-1990_02 |