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HRID12051

反应详情

EQUATION

反应方程式

HRID 12051 的结构方程式

REACTANTS

反应物

2
结构：Fc1ccc(C2=CCC3(CC2)OCCO3)cc1
HCID15232682

8-(4-Fluorophenyl)-1,4-dioxaspiro[4.5]dec-7-ene

C14H15FO2

结构：[H][H]
HCID178418361

未命名化合物

PRODUCTS

生成物

1
结构：Fc1ccc(C2CCC3(CC2)OCCO3)cc1
HCID12834404

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]dec-7-ene is hydrogenated using Pd/C with hydrogen. After filtering-off of the catalyst over celite and evaporating-off of the solvent, 8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]decane is obtained in a quantitative yield: tR 3.65 min (LC-1); ESI-MS(+): m/z 237.26 [M+H]+.