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HRID12247

反应详情

EQUATION

反应方程式

HRID 12247 的结构方程式

REACTANTS

反应物

2
结构：CC1CNCC(C)O1
HCID110862

2,6-Dimethyl morpholine

C6H13NO

结构：CC1(C)CN(CC(=O)O)C(C(=O)Nc2cc(Cl)cc3c2[nH]c2cnccc23)CO1
HCID59337527

未命名化合物

PRODUCTS

生成物

1
结构：CC1CN(C(=O)CN2CC(C)(C)OCC2C(=O)Nc2cc(Cl)cc3c2[nH]c2cnccc23)CC(C)O1
HCID67165125

未命名化合物

PROCEDURE

实验过程

The desired compound was prepared using [5-(6-Chloro-9H-beta-carbolin-8-ylcarbamoyl)-2,2-dimethyl-morpholin-4-yl]-acetic acid and 2,6-dimethyl morpholine following Method F. Chromatographic purification gave the desired product in 70-80% yield.

WORKUP

后处理

  1. customThe desired compound was prepared
  2. customChromatographic purification