HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Tert-butylcyclohexanecarbonyl chloride → 4-tert-butyl-N-[1-(3-tert-butyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclohexanecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Tert-butylcyclohexanecarbonyl chloride | HCID 2757269 | — |
| Reactant | 6-(1-Aminopropyl)-3-tert-butyl-1,2,4-triazin-5(4h)-one | HCID 135594090 | — |
| Product | 4-tert-butyl-N-[1-(3-tert-butyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclohexanecarboxamide | HCID 135594089 | — |
Reaction Steps
In analogy to the procedure for Example 36A, 210 mg (1.00 mmol) 6-(1-aminopropyl)-3-tert-butyl-1,2,4-triazin-5(4H)-one, 200 mg (1.00 mmol) 4-tert-butylcyclohexanecarbonyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115602B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-7430f96f69964f2dae79215de9da8d9e |
| Source note | uspto-grants-2006_10 |