Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia methanol | HCID 21705897 | — |
| Reactant | HCID 54720306 | HCID 54720306 | — |
| Product | HCID 54720309 | HCID 54720309 | 7.5% |
Reaction Steps
A mixture of intermediate 19 (20 g; 82 mmol) in CH3OH/NH3 (150 ml) was stirred at 60° C. for 4 hours, evaporated till dryness and taken up in diisopropyl ether. The precipitate was filtered to yield 1.5 g of intermediate 20 (7.5%). The product was used without further purification in the next reaction step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07115608B2 |
|---|
| Source dataset | uspto-grants-2006_10 |
|---|
| ORD ID | ord-c9f8ea7d31ae4c848fed09e724a76ca0 |
|---|
| Source note | uspto-grants-2006_10 |
|---|
