HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 10023837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 21935301 | HCID 21935301 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10023837 | HCID 10023837 | — |
Reaction Steps
NaBH4 (0.047 g; 1.3 mmol) was added to a mixture of compound 159 (0.5 g; 0.013 mol) in methanol (3 ml). The mixture was stirred at room temperature for 1 hour. Water was added. The precipitate was filtered off, taken up in diisopropyl ether and dried to yield 0.26 g (52%), m.p.=70° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115608B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-ef09482df842418ca62e8f31c693545b |
| Source note | uspto-grants-2006_10 |