HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 54720303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69640128 | HCID 69640128 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54720303 | HCID 54720303 | — |
Reaction Steps
A mixture of intermediate 24 (0.1 g; 0.003 mol) and sodium hydroxide (0.038 g; 0.0009 mol) in H2O (1.5 ml) was stirred and refluxed for 15 hours, then cooled to 5° C. with HCl 3N. The precipitate was filtered, washed with H2O, then with isopropanol and dried to yield 0.07 g (91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115608B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-55452cd664a643c584e78591ec2c94b1 |
| Source note | uspto-grants-2006_10 |