1,3-Benzodioxol-4-amine → HCID 21936009, compound

Participants

Reaction Steps

Using an analogous procedure to that described in Example 1, 4-chloro-6,7-di-(2-methoxyethoxy)quinazoline (U.S. Pat. No. 5,747,498; 0.1 g) was reacted with 2,3-methylenedioxyaniline (0.048 g) to give the title compound (0.121 g); NMR Spectrum: (DMSOd6 and CF3CO2D) 3.5 (s, 6H), 3.8 (m, 4H), 4.35 (m, 4H), 6.05 (s, 2H), 6.95 (m, 3H), 7.4 (s, 1H), 8.2 (s, 1H), 8.85 (s, 1H); Mass Spectrum: M+H+ 414.

Provenance & Evidence