HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum(III) Chloride → HCID 178479874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 11035407 | HCID 11035407 | — |
| Reactant | HCID 21936568 | HCID 21936568 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 178479874 | HCID 178479874 | 88% |
Reaction Steps
The general procedure (Method K) applied to 3-chloro-6-methoxy-8-methyl-8H-quino[4,3,2-kl]acridine, 32 (5.5 g, 15.9 mmol), with aluminium chloride (6.3 g, 3 eq), and benzene (500 ml) gave the title compound as a yellow solid (4.5 g, 13.5 mmol, 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115619B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-8bca587a434546eb957ad5ba8163dcb2 |
| Source note | uspto-grants-2006_10 |