HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoromethanesulfonic anhydride → HCID 11145051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoromethanesulfonic anhydride | HCID 67749 | — |
| Reactant | HCID 178479883 | HCID 178479883 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11145051 | HCID 11145051 | 81% |
Reaction Steps
The general procedure (Method L) applied to trifluoromethanesulphonic acid anhydride (0.05 ml, 0.3 mmol, 1 eq), 10-chloro-6-hydroxy-8-methyl-8H-quino[4,3,2-kl]acridine, 37 (100 mg, 0.3 mmol) in DCM (50 mL) gave the title compound as a yellow solid, (114 mg, 0.25 mmol, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115619B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-ec5233da71524c36bd618d73ccec8fbd |
| Source note | uspto-grants-2006_10 |