Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxyamine hydrochloride → 2-Chloro-6-(4-pyridyl)benzaldoxime
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 반응물 | 2-Chloro-6-(4-pyridyl)benzaldehyde | HCID 21937646 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2-Chloro-6-(4-pyridyl)benzaldoxime | HCID 136334122 | 99% |
반응 단계
2-Chloro-6-(4-pyridyl)benzaldehyde (80 mg, 0.37 mmol) was dissolved in pyridine (2 mL) at room temperature. Hydroxylamine hydrochloride (26 mg, 0.38 mmol) was added and the mixture was allowed to stir overnight. The mixture was then concentrated under reduced pressure to obtain 2-chloro-6-(4-pyridyl)benzaldoxime (85 mg, 99% yield). MW=233 confirmed by LC-MS, tr=8.36 min (Method Y) MH+=231–235
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07115642B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-6826822b0fac4c448f64999aae1ecf01 |
| 출처 메모 | uspto-grants-2006_10 |