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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1242637Generated: October 31, 2026

Allyl Isothiocyanate → HCID 21939689, compound

https://huagongshe.com/reaction/1242637

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl IsothiocyanateHCID 5971—
ReactantHCID 21939690HCID 21939690—
SolventBromobenzeneHCID 7961—
ProductHCID 21939689HCID 2193968986.8%

Reaction Steps

. . A solution of 140 mg (1.0 mmol) of 2-thienyl-1,2-diaminoethane and allyl isothiocyanate (99 mg, 1 mmol) in bromobenzene (5 mL) was heated for 40 min and allowed to cool to room temperature and then cooled to −5° C. The title compound (160 mg, 83% yield) was obtained upon filtration and washing with hexane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07115748B2
Source datasetuspto-grants-2006_10
ORD IDord-3927865a6d224dd38741e6960fa630da
Source noteuspto-grants-2006_10