HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl Isothiocyanate → HCID 21939689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl Isothiocyanate | HCID 5971 | — |
| Reactant | HCID 21939690 | HCID 21939690 | — |
| Solvent | Bromobenzene | HCID 7961 | — |
| Product | HCID 21939689 | HCID 21939689 | 86.8% |
Reaction Steps
. . A solution of 140 mg (1.0 mmol) of 2-thienyl-1,2-diaminoethane and allyl isothiocyanate (99 mg, 1 mmol) in bromobenzene (5 mL) was heated for 40 min and allowed to cool to room temperature and then cooled to −5° C. The title compound (160 mg, 83% yield) was obtained upon filtration and washing with hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115748B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-3927865a6d224dd38741e6960fa630da |
| Source note | uspto-grants-2006_10 |