Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21917012 | HCID 21917012 | — |
| Product | HCID 21917244 | HCID 21917244 | — |
Reaction Steps
The product obtained in Step B (3 mmol), dissolved in thionyl chloride, is stirred at 60° C. under a current of nitrogen for one hour. The thionyl chloride is evaporated off under reduced pressure and the residue is dried with the aid of a vane pump to yield the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07115752B2 |
|---|
| Source dataset | uspto-grants-2006_10 |
|---|
| ORD ID | ord-d6713289d7784bf3926cf52e2160513a |
|---|
| Source note | uspto-grants-2006_10 |
|---|
