HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 2-[4-benzylpiperazinyl]benzoate → Methyl 2-(piperazin-1-yl)benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 2-[4-benzylpiperazinyl]benzoate | HCID 21935101 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Produkt | Methyl 2-(piperazin-1-yl)benzoate | HCID 10932975 | — |
Reaktionsschritte
The title compound was prepared according to the procedure described in Preparation IV by using methyl 2-[4-benzylpiperazinyl]benzoate (2.8 g, 8.9 mmol), 10% Pd/C (Aldrich) (940 mg), and HCO2NH4 (2.8, 44 mmol). The title compound was isolated as a colorless oil (1.75 g). (MS (ESI, pos. ion) m/z: 221 (M+H). Calc'd for C12H16N2O2: 220.12.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07115607B2 |
| Quelldatensatz | uspto-grants-2006_10 |
| ORD ID | ord-55c106eb892f453d8308f4bfaa0b7ffa |
| Quellennotiz | uspto-grants-2006_10 |