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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1242900Generated: November 1, 2026

Dimethylformamide dimethyl acetal → HCID 21939863, compound

https://huagongshe.com/reaction/1242900

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
ReactantN-(1-Oxo-2,3-dihydro-1H-inden-5-yl)acetamideHCID 312894—
ProductHCID 21939863HCID 21939863—

Reaction Conditions

Temperature100 °C

Reaction Steps

Dimethylformamide dimethylacetal was added to 5-acetamido-1-indanone (2.5 g, 13.2 mmol), which was stirred at 100° C. for 3.5 hours, and cooled to room temperature. The precipitated crude products were collected, which was washed with ethyl acetate to give the titled compound (2.73 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07115750B1
Source datasetuspto-grants-2006_10
ORD IDord-8e459ffcea8549cabb7946ba3da3ae7f
Source noteuspto-grants-2006_10