(2-(Trifluoromethoxy)phenyl)methanamine → 5-Bromo-2-(4-chloro-benzenesulfonylamino)-N-(2-trifluoromethoxy-benzyl)-benzamide

Participants

Reaction Steps

This compound was prepared using the procedure described in Example 70, using 5-bromo-2-(4-chloro-benzenesulfonylamino)-benzoyl chloride instead of 5-bromo-2-(4-trifluoromethoxy-benzenesulfonylamino)-benzoyl chloride, and 2-trifluoromethoxybenzyl amine instead of 2-methoxy benzyl amine. M/Z of [M−H]−=563.8. 1H NMR (DMSO) δ=4.4 (sd, 2H), 7.3–7.4 (5H), 7.5 (2H), 7.65–7.7 (3H), 7.9–8.0 (1H), 9.4 (br, 1H), 11.5 (br, 1H).

Provenance & Evidence