HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178519336, compound → HCID 178519335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178519336 | HCID 178519336 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178519335 | HCID 178519335 | 99.1% |
Reaction Steps
(2-Phenyl-1H-benzoimidazol-5-yl)-methanol (783 mg, 3.49 mmol) was dissolved in 20 mL THF. Added MnO2 (3.035 g, 34.91 mmol) and stirred at RT for 1 hour. Filtered through celite and removed solvent in vacuo. Obtained 769 mg (99.1%) of 2-Phenyl-1H-benzoimidazole-5-carbaldehyde as a light yellow foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07119102B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-fdc91b2e07b543a296cf12288a350966 |
| Source note | uspto-grants-2006_10 |