HRID1243803

反应详情

EQUATION

反应方程式

HRID 1243803 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

(2-Phenyl-1H-benzoimidazol-5-yl)-methanol (783 mg, 3.49 mmol) was dissolved in 20 mL THF. Added MnO2 (3.035 g, 34.91 mmol) and stirred at RT for 1 hour. Filtered through celite and removed solvent in vacuo. Obtained 769 mg (99.1%) of 2-Phenyl-1H-benzoimidazole-5-carbaldehyde as a light yellow foam.

WORKUP

后处理

  1. filtrationFiltered through celite
  2. customremoved solvent in vacuo