Chloroform → HCID 58709433, compound

Participants

Reaction Steps

Briefly, 4,4′,6,6′-tetra(chloro)hydrazo-1,3,5-triazine (1) [9] reacts rapidly with an excess of hydrazine monohydrate in acetonitrile to give 4,4′,6,6′-tetra(hydrazino)-hydrazo-1,3,5-triazine (2). Compound (2) undergoes diazotization to yield 4,4′,6,6′-tetra(azido)hydrazo-1,3,5-triazine (3). A suspension of (3) in 1:2 (v/v) H2O:CHCl3 solution reacts with chlorine gas at room temperature to provide 4,4′,6,6′-tetra(azido)azo-1,3,5-triazine (4, TAAT).

Provenance & Evidence