HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 21928838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 21929019 | HCID 21929019 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21928838 | HCID 21928838 | — |
Reaction Steps
But starting with 0.3 g of 6,6-diphenyl-1-(4-toluenesulphonyl)-6,7-dihydro-1H-indazole-3ylamine, 0.095 cm3 of triethylamine and 0.088 cm3 of benzoyl chloride in cm3 of dichloromethane. After flash chromatography on a column of silica [eluent: dichloromethane], 0.14 g of N-(6,6-diphenyl-6,7-dihydro-1H-indazol-3-yl)benzamide is thus obtained in the form of a foam, the characteristics of which are as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07119115B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-684d9677a55244e2ac6bbe86f591c6b2 |
| Source note | uspto-grants-2006_10 |