Reserpine → HCID 10285937, compound

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Reaction Steps

The title compound was prepared according to the procedure used for the preparation of 6-cyclopropyl-1-methyl-2-oxo-1,2,3,4-tetrahydro-quinoline-7-carbaldehyde as a yellow solid. 1H NMR (400 MHz, CDCl3) δ 1.47 (3H, t, J=7.0 Hz), 2.65 (2H, m), 2.93 (2H, m), 3.36 (3H, s), 4.14 (2H, q, 7.1 Hz), 6.81 (1H, s), 7.42 (1H, s), 10.45 (1H, s). m/z (APCI+) 233.9 (M+1). HPLC (aqueous 200 Mm ammonium acetate buffer/acetonitrile gradient, 3.0 ml/min, Hewlett Packard ODS Hypersil 5 μM, 125×4 mm column), 4.167 min.

Provenance & Evidence