Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 9995922 | HCID 9995922 | — |
| Product | HCID 10406543 | HCID 10406543 | — |
Reaction Steps
A mixture of 6-chloro-4-ethyl-3-[2-(3-fluoro-phenyl)-imidazol-1-ylmethyl]-pyridazine (55.3 mg, 0.17 mmol) and piperidine (5 mL) is heated at 110° C. for 5 hours. Excess piperidine is removed and the residue is purified by PTLC to give the title compound. LC-MS (M+1) 366.2 (retention time: 0.91 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07122546B2 |
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| Source dataset | uspto-grants-2006_10 |
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| ORD ID | ord-3a58f62abcc14587963d3c3ce2163728 |
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| Source note | uspto-grants-2006_10 |
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