Dimethylamine → HCID 178492005, compound

Participants

Reaction Conditions

Reaction Steps

0.03 g 5-Chloro-2-(4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-3H-imidazo[4,5-b]pyridine (0.07 mmol) was dissolved in dimethylamine (5 ml) in an autoclave and heated to 200° C. for 16 h. The residue was triturated in water whereupon a precipitate formed, which was isolated and dried in vacuo. 0.08 g [2-(4-Methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-3H-imidazo[4,5-b]pyridin-5-yl]-dimethyl-amine (29%) were obtained as a brown solid; M.p.: 120–130° C.

Provenance & Evidence