反应详情

6.54 g 4-Azido-5-hydroxy-azepane-1-carboxylic acid tert-butyl ester in 51 ml methanol were hydrogenated in the presence of 0.6 g palladium on charcoal (10%) to yield 5.85 g (quant.) 4-amino-5-hydroxy-azepane-1-carboxylic acid tert-butyl ester as viscous oil; MS (ISP): m/e=231 (M+H+).