HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylglyoxal → 3-(4-Fluoro-benzyl)-7-phenyl-[1,2,4]triazolo[4,3-b][1,2,4]triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylglyoxal | HCID 14090 | — |
| Reactant | 5-[(4-Fluorophenyl)methyl]-4H-1,2,4-triazole-3,4-diamine | HCID 21919322 | — |
| Product | 3-(4-Fluoro-benzyl)-7-phenyl-[1,2,4]triazolo[4,3-b][1,2,4]triazine | HCID 21919317 | — |
Reaction Steps
General procedure A was followed with the reaction of oxo-phenyl-acetaldehyde and 5-(4-fluoro-benzyl)-[1,2,4]triazole-3,4-diamine to provide 3-(4-fluoro-benzyl)-7-phenyl-[1,2,4]triazolo[4,3-b][1,2,4]triazine and the desired product 3-(4-fluoro-benzyl)-6-phenyl-[1,2,4]triazolo[4,3-b][1,2,4]triazine (example 4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122548B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-61c720a8e1f049ccae42ee87b9b460c5 |
| Source note | uspto-grants-2006_10 |