4-Bromobenzaldehyde → HCID 69123853, compound

HRID 1244664Notes

Reaction equation

HRID 1244664 reaction equation
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.Cl.[S:11]([C:15]1[CH:20]=[CH:19][C:18]([NH:21][NH2:22])=[CH:17][CH:16]=1)(=[O:14])(=[O:13])[NH2:12]>>[S:11]([C:15]1[CH:16]=[CH:17][C:18]([NH:21][N:22]=[CH:6][C:5]2[CH:8]=[CH:9][C:2]([Br:1])=[CH:3][CH:4]=2)=[CH:19][CH:20]=1)(=[O:14])(=[O:13])[NH2:12]

Participants

3

Reactant 2

HCID 707414-BromobenzaldehydeHCID 27945674-Hydrazinylbenzenesulfonamide hydrochloride

Product 1

HCID 69123853HCID 69123853, compoundYield 66%

Procedure

A solution of 4-bromobenzaldehyde (5 mmol) and 4-sulfamylphenyl-hydrazine hydrochloride was subjected to the General Procedure. The title compound, melting point 190–192° C., was obtained in 66% yield.

Sources & evidence

ORD record
ord-e8b5fa889657405c9a97c5a82e8dd5f0
Source dataset
uspto-grants-2006_10
Patent number
US07122571B2

Reaction notes

Loading…