4-Methoxybenzaldehyde → HCID 3765022, compound

HRID 1244665Notes

Reaction equation

HRID 1244665 reaction equation
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.Cl.[S:12]([C:16]1[CH:21]=[CH:20][C:19]([NH:22][NH2:23])=[CH:18][CH:17]=1)(=[O:15])(=[O:14])[NH2:13]>>[S:12]([C:16]1[CH:17]=[CH:18][C:19]([NH:22][N:23]=[CH:7][C:6]2[CH:9]=[CH:10][C:3]([O:2][CH3:1])=[CH:4][CH:5]=2)=[CH:20][CH:21]=1)(=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 312444-MethoxybenzaldehydeHCID 27945674-Hydrazinylbenzenesulfonamide hydrochloride

Product 1

HCID 3765022HCID 3765022, compoundYield 62%

Procedure

A solution of 4-methoxybenzaldehyde (5 mmol) and 4-sulfamylphenyl-hydrazine hydrochloride was to the General Procedure. The title compound, melting point 228–231° C., was obtained in 62% yield.

Sources & evidence

ORD record
ord-3151dbd1d8b4444893dfd8cddb051f7d
Source dataset
uspto-grants-2006_10
Patent number
US07122571B2

Reaction notes

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