2-Acetylthiophene → HCID 75953104, compound
Reaction equation
[C:1]([C:4]1[S:5][CH:6]=[CH:7][CH:8]=1)(=O)[CH3:2].Cl.[S:10]([C:14]1[CH:19]=[CH:18][C:17]([NH:20][NH2:21])=[CH:16][CH:15]=1)(=[O:13])(=[O:12])[NH2:11]>>[S:10]([C:14]1[CH:15]=[CH:16][C:17]([NH:20][N:21]=[C:1]([C:4]2[S:5][CH:6]=[CH:7][CH:8]=2)[CH3:2])=[CH:18][CH:19]=1)(=[O:13])(=[O:12])[NH2:11]Participants
3
Procedure
A solution of 2-acetylthiophene (5 mmol) and 4-sulfamylphenylhydrazine hydrochloride is subjected to the General Procedure. The title compound is isolated as described in the general procedure.
Sources & evidence
- ORD record
- ord-2b6b99b7a81b45e4818c45a8797de9d8
- Source dataset
- uspto-grants-2006_10
- Patent number
- US07122571B2
Reaction notes
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